Abstract
Fast neutron-activation methods have been developed for the determination of iron and silicon in USGS and Indian standards and bauxites. Nuclear reactions56Fe/n, p/56Mn and28Si/n, p/28Al were carried out using241Am-Be neutron source and cutting off thermal neutrons with a Cd shield. For Si a cyclic method was adopted due to short half life of28Al /2.3 min/. The methods are non destructive, fast, economic and ideal for bulk analysis of rocks and process control.
Similar content being viewed by others
References
C.S. Sastri,Nucl. Instr. Methods Phys. Res., 221 /1984/ 566.
S. Amiel, Ed. Non-destructive Activation Analysis with Nuclear Reactors and Radioactive Neutron Sources; Studies in Analytical Chemistry, Vol. 3, Elsevier, Amsterdam, 1981, p. 369.
A.N. Garg, R.J. Batra,J. Radioanal. Nucl. Chem., 98 /1986/ 167.
J.I.W. Watterson, A.N. Andeweg, J. Ramanlo,J. Radioanal. Chem., 71 /1982/ 365.
R.J. Holmes, M. Borsaru, A.W. Wylie, The Aus. I.M.M. Conf. North Queensland, 1978, p. 1.
R.J. Holmes, A.J. Messenger, J.G. Miles,Proc. Aust. Inst. Min. Metall., 274 /1980/ 17.
M. Borsaru, R.J. Holmes, P.J. Mathew,Int. J. Appl. Radiat. Isotopes, 34 /1983/ 397.
R.J. Holmes,Anal. Chem., 48 /1976/ 1155.
L. Alaerts, J.P. Op. De Beeck, J. Hoste,Anal. Chim. Acta, 73 /1974/ 53.
M. Borsaru, P.J. Mathew,Anal. Chim. Acta, 142 /1982/ 349.
L. Alaerts, J.P. Op. De Beeck, J. Hoste,Anal. Chim. Acta, 78 /1975/ 329.
M. Borsaru, P.L. Eisler,Anal. Chem., 53 /1981/ 1751.
A.N. Garg,Radiochem. Radioanal. Lett., 39 /1979/ 319.
H. Tominaga, T. Imahashi, S. Enomoto, N. Tachikawa, M. Maeda, K. Itakura,J. Radioanal. Chem., 50 /1979/ 235.
I. Çelenk F. Özek,J. Radioanal. Nucl. Chem. Lett., 85 /1984/ 83.
M. Borsaru, R.J. Holmes,Anal. Chem., 50 /1978/ 296.
R.J. Batra, A.N. Garg,Ind. J. Chem., 25A /1986/
B.T. Kenna, P.E. Harrison, Sandia Laboratories Research, Report SLA-73-0637, 1973, p. 90.
I.M.H. Pagden, G.J. Pearson, J.M. Bewers, An Isotope Catalogue for Instrumental Activation Analysis,J. Radioanal. Chem., 8 /1971/ 127.
A.I. Vogel, Textbook of Quantitative Inorganic Analysis, 4th Edition, Longman, London, 1978, pp. 466, 742, 503, 757.
F.J. Flanagan,Geochim. Cosmochim. Acta, 37 /1973/ 1189.
J.C. Laul, N.A. Wogman, in Trace Analysis and Technological Development, Ed. M. Sankar Das, Wiley Eastern Ltd., New Delhi, 1983, p. 218.
G.R. Reddy, D.R. Pant, B.L. Rao, M. Sankar Das,J. Radioanal. Chem., 33 /1976/ 39.
S. Gangadharan, S.Y. Subramanian,J. Radioanal. Chem., 42 /1978/ 455.
P.B. Pawaskar, B.S. Manerkar, M. Sankar Das,J. Geol. Soc. India, 26 /1985/ 219.
R. Dybczynski, A. Tugsavul, O. Suschny, Report on Soil-5 for the Determination of Trace Elements in Soil, IAEA/RL/46, 1978.
Author information
Authors and Affiliations
Rights and permissions
About this article
Cite this article
Batra, R.J., Lanjewar, R.B. & Garg, A.N. NAA determiantion of iron and silicon in USGS standards and bauxites using fast neutrons from241Am-Be source. Journal of Radioanalytical and Nuclear Chemistry Letters 104, 115–125 (1986). https://doi.org/10.1007/BF02166926
Received:
Accepted:
Issue Date:
DOI: https://doi.org/10.1007/BF02166926