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Effect of gamma-radiation on amorphous mixed zirconium-titanium phosphates

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Abstract

A precipitation method was used to prepare amorphous mixed zirconium-titanium phosphates with various titanium contents. In this way the acidic solutions of ZrOCl2.8H2O and TiCl4 in various ratios were rapidly mixed with a phosphoric acid solution under continuous stirring. The resulting precipitate, characterized as [ZrxTi/1−x//HPO4/2.n H2O] was contacted with water of ethanol, then washed to pH ∼3.0 and dried at room temperature. The samples were irradiated with γ-rays of a60Co source giving a 6.6×107 Gy total dose. The thermal, chemical and ion-exchange properties of irradiated samples were investigated.

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Authors and Affiliations

  1. Basic Science Research Center, Al-Fateh Universities Campus, P. O. Box 13439, Tripoli, Great Jamahiriya /GSPLAJ/

    S. K. Shakshooki

  2. Institute of Isotopes of the Hungarian Academy of Sciences, P. O. Box 77, H-1525, Budapest, Hungary

    L. Szirtes

Authors
  1. S. K. Shakshooki
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  2. L. Szirtes
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Shakshooki, S.K., Szirtes, L. Effect of gamma-radiation on amorphous mixed zirconium-titanium phosphates. Journal of Radioanalytical and Nuclear Chemistry Letters 137, 159–166 (1989). https://doi.org/10.1007/BF02164578

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  • DOI: https://doi.org/10.1007/BF02164578

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