Summary
The qualitative and quantitative analysis of synthetic mixtures of non-isomeric and isomeric methylated glucoses, as present in the hydrolysate of methylated glucopolysaccharides, has been achieved by hydrogenation of the methylated sugars to the corresponding methylated hexitols, esterification withp-azobenzoylchlorid, and chromatographic analysis on activated alumina.
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Boissonnas, R.A. Séparation chromatographique de sucres méthylés isomères. Experientia 3, 238–239 (1947). https://doi.org/10.1007/BF02164139
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DOI: https://doi.org/10.1007/BF02164139