Abstract
A key aspect of the development of a procedure for the measurement of technetium in environmental samples is that each step should be optimized to achieve maximum recovery.99Tc and95mTc have been the tracers used for the determination of yields in steps involving anion exchange, leaching, ashing, solvent extraction, precipitation and evaporation. The results thus obtained are discussed.
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References
A.G. Jones, A. Davison,J. Appl. Radiat. Isot., 33 (1982) 867.
J.H. Kaye, J.A. Merrill, P.R. Kinnison, M.S. Rapids, N.E. Ballou,Anal. Chem., 54 (1982) 1158.
S.E. Long, S.T. Sparkes, AERE-R 12742, 1988.
K.V. Kotegov, O.N. Pavlov, V.P. Shvedo,Advances in Inorg. Chem. Radiochem., 11 (1968) 1.
A.K. Lavrukhina, A.A. Pozdnyakov, (Eds), Analytical Chemistry of Technetium, Promethium, Astatine and Francium (Transl. by R. Kondor) Ann Arbor-Humphrey Science, London, 1970.
E. Anders, The Radiochemistry of Technetium, NAS-NS 3021, U.S. Dept. of Commerce, Springfield, Virginia, 1960.
T.J. Anderson, R.L. Walker,Anal. Chem., 52 (1980) 709.
Q. Chen, H. Dahlgaard, H.J.M. Hansen, A. Aarkrog,Anal. Chim. Acta., 228 (1990) 163.
C. Hurtgen, G. Koch, D. Van Der Ben, A. Bonotto,Sci. Tot. Environ., 70 (1988) 131.
M. Koide, E.D. Goldberg,J. Environ. Radioact., 2 (1985) 167.
J. Rioseco,99Tc, Dotoral dissertation, University of Lund, Sweden, 1987.
E. Holm, J. Rioseco, M. Garcia-Leon,Inst. Meth. Phys. Res., 223 (1984) 204.
N. Momoshima, N. Inoue, Y. Takashima,J. Radioanal. Nucl. Chem., 155 (1991) 335.
Q. Chen, A. Aarkrog, H. Dahlgaard, S.P. Nielsen, E. Holm, H. Dick, K. Mandrup,J. Radioanal. Nucl. Chem., 131 (1989) 171.
P. Robb, Ph.D. Thesis, Loughborough University, U.K., 1983.
S. Foti, E. Delucchi, V. Akamian,Anal. Chim. Acta., 60 (1972) 269.
Ihsanullah, Ph.D. Thesis, Glasgow University, U.K., 1991.
A.R. Date, A.L. Gray, Applications of Inductively Coupled Plasma Mass-Spectrometry, (1st edn), Blackie, Glasgow, U.K., 1989.
B.R. Harvey, K.J. Williams, M.B. Lovett, R.D. Ibbett,J. Radioanal. Nucl. Chem., 228 (1992) 417.
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Ihsanullah Losses of technetium during various steps in the development of a procedure for environmental samples. Journal of Radioanalytical and Nuclear Chemistry Letters 176, 303–313 (1993). https://doi.org/10.1007/BF02163495
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DOI: https://doi.org/10.1007/BF02163495