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Die isolierung von 17β-hydroxyandrost-4-en-3-on-17-sulfat (testosteronsulfat) aus männlichem Urin

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Summary

Testosterone sulphate has been isolated from the urine of a normal male subject. The characterization of the substance was based upon the following criteria: Identical Rf values of authentic testosterone sulphate and of the unknown compound in the paperchromatographic systemSi; positive methylene blue-reaction and UV contact photogram; identical absorption spectra in concentrated sulphuric acid. Following dioxan solvolysis, only testosterone has been detected. Epitestosterone could not been found.

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Authors and Affiliations

  1. Hormonlabor, 2. Medizinische Universitätsklinik, Hamburg, Deutschland

    J. Tamm, U. Volkwein & K. D. Voigt

Authors
  1. J. Tamm
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  2. U. Volkwein
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  3. K. D. Voigt
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Additional information

Die in der Arbeit dargestellten Experimente wurden durch die Deutsche Forschungsgemeinschaft unterstützt. Testosteronsulfat wurde dankenswerterweise durch die Merck A.G., Darmstadt, zur Verfügung gestellt.

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Tamm, J., Volkwein, U. & Voigt, K.D. Die isolierung von 17β-hydroxyandrost-4-en-3-on-17-sulfat (testosteronsulfat) aus männlichem Urin. Experientia 23, 299–300 (1967). https://doi.org/10.1007/BF02135699

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  • DOI: https://doi.org/10.1007/BF02135699

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