Skip to main content
SpringerLink
Log in

Determination of liquid vapour adsorption and desorption on and from solids by means of the derivatograph

Part I. Derivatograph for measurements of adsorption and desorption at a constant temperature

  • Published:
Journal of thermal analysis Aims and scope Submit manuscript

Abstract

A modofied Q-1500 D derivatograph (MOM, Hungary) allowing measurements of sample weight changes at constant temperature is described. The sample weight changes measured were due to the adsorption and desorption of liquid vapour flowing in an inert gas stream through the measuring cell at constant temperature. This apparatus permits the utilization of thermal analysis for adsorption investigations.

Zusammenfassung

Es wird ein modifizierter Derivatograph vom Typ Q-1500 D (MOM, Ungarn) beschrieben, der die Messung von Veränderungen des Probengewichtes bei konstanter Temperatur ermöglicht. Die adsorption und Desorption einer bei konstanter Temperatur in einem inerten Gasstrom durch die Meßzelle strömenden gasförmigen Substanz wird durch Messung des Probengewichtes verfolgt. Eine Apparatur für thermische Analyse wird damit zu Adsorptionsuntersuchungen verwendet.

Резюме

Описан модифицирова нный дериватограф ти па Q-1500 Д (MOM, Венгрия), позволяющий проводи ть измерения изменен ий веса образца при постоянн ой температуре. За весовыми изменениям и следует адсорбция и десорбция паров, находящихса в п отоке инертного газа и пропускаемых ч ерез измерительную я чейку при постоянной темлерат уре. Аппаратура дает возможность исп ользовать метод терм ического анализа для исследов ания адсорбции.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

References

  1. J. Paulik and F. Paulik: Simulateneous Thermoanalytical Examinations by Means of the Derivatograph; in the series Wilson and Wilson's Comprehensive Analytical Chemistry (ed. by G. Svehla), Vol. XII. Advisory editor W. W. Wendlandt, Elsevier, Amsterdam, 1981.

    Google Scholar 

  2. D. Schultze, Differential Thermal Analysis, PWN, Warsaw, 1974.

    Google Scholar 

  3. L. Stoch, Clay Minerals, Wyd. Geologiczne, Warsaw, 1974.

    Google Scholar 

  4. P. Gill, International Laboratory, 4 (1984) 78.

    Google Scholar 

  5. J. Simon, J. Thermal Anal., 4 (1972) 205.

    Google Scholar 

  6. L. Stoch, Problems of Thermal Analysis, Wyd. Geologiczne, Warsaw, 1972, p. 7.

    Google Scholar 

  7. V. Dondur and D. Vucelić, Thermochim. Acta, 68 (1983) 91.

    Google Scholar 

  8. A. M. Arjona and M. A. L. Franco, J. Thermal Anal., 5 (1973) 319.

    Google Scholar 

  9. P. Staszczuk, Apparatus for Measurement of Adsorption and Desorption of Liquids on Solid Surfaces, Patent No. P-249986 (1984), submitted to Polish Patent Office.

Download references

Author information

Authors and Affiliations

  1. Department of Physical Chemistry, Institute of Chemistry, Maria Curie-Sklodovska University, M. Curie-Sklodovska SQ. 3, 20-031, Lublin, Poland

    P. Staszczuk

Authors
  1. P. Staszczuk
    View author publications

    You can also search for this author in PubMed Google Scholar

Rights and permissions

Reprints and permissions

About this article

Cite this article

Staszczuk, P. Determination of liquid vapour adsorption and desorption on and from solids by means of the derivatograph. Journal of Thermal Analysis 30, 1115–1119 (1985). https://doi.org/10.1007/BF02108542

Download citation

  • Received:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF02108542

Keywords

Search

Navigation