Abstract
Mössbauer measurements have been performed in situ in the temperature range of 25 to 550°C for three Cr-Fe samples: Cr72Fe28 crystalline alloy (I), as-milled amorphous Cr65Fe35 powders made by mechanical grinding (II) and the same powder annealed at 420°C for 2 h (III). The temperature dependence of isomer shifts for samples I and III follows the variation predicted by the second-order Doppler effect, while for the sample II a deviation has been observed. The Debye temperatures have been determined to be 420, 400 and 380 K for sample I, III and II, respectively. A linear dependence onT 3/2 of quadrupole splitting of the annealed powder is observed.
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Xia, S.K., Baggio-Saitovitch, E. Dynamical properties of Cr-Fe amorphous powders obtained from mechanical milling. Hyperfine Interact 83, 267–270 (1994). https://doi.org/10.1007/BF02074283
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DOI: https://doi.org/10.1007/BF02074283