Skip to main content
Log in

Effect of helium environment and mylar foil on the sensitivity of different elements in energy dispersive X-ray fluorescence spectroscopy

  • Published:
Journal of Radioanalytical and Nuclear Chemistry Aims and scope Submit manuscript

Abstract

Analysis by Energy Dispersive X-Ray Fluorescence (ED-XRF) technique of liquid samples and specimens in aqueous media requires that the sample chamber be flushed with helium gas. Moreover the sample should also be covered with mylar foil to hold the sample. The helium environment and the X-ray beam but also affect the sensitivity of different elements. An investigation was carried out with six multielement NBS standards to evaluate the effect of helium environment and mylar foil on the sensitivity of various elements. The effect of both the factors can be employed to improve the results of liquid samples with ED-XRF technique.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. I. M. SZOGHY, C. POLIQUIN, X-Ray Spectrom., 10 (1981) 69.

    Article  Google Scholar 

  2. A. M. HARRIS, D. F. BAINES, X-Ray Spectrom., 5 (1976) 129.

    Article  Google Scholar 

  3. G. E. PURDUE, R. W. WILLIAMS, X-Ray Spectrom., 14 (1985) 102.

    Article  Google Scholar 

  4. P. K. ROKOSZ, B. E. ARTZ, R. K. BELITZ, Adv. X-Ray Anal., 28 (1985) 177.

    Google Scholar 

  5. P. K. KOUL, B. D. PADALIA, X-Ray Spectrom., 12 (1983) 128.

    Article  Google Scholar 

  6. J. A. LARSON, M. A. SHORT, S. BONFIGLIO, W. ALLIE, X-Ray Spectrom., 3 (1974) 125.

    Article  Google Scholar 

  7. G. R. WATERBURY, E. A. HAKKILA, Anal. Chem., 37 (1965) 1773.

    Article  Google Scholar 

  8. C. W. DWIGGINS, Anal. Chem., 36 (1964) 1577.

    Article  Google Scholar 

  9. J. E. van ENK, J. JANSSEN, W. K. de JONGH, X-Ray Spectrom., 5 (1976) 68.

    Article  Google Scholar 

  10. S. BRONTMAN, Edax Editor, 14 (1983) 13.

    Google Scholar 

  11. C. C. KANG, E. E. KELL, E. SOLOMON, Anal. Chem., 32 (1960) 221.

    Article  Google Scholar 

  12. M. LAL, R. K. CHOUDHURY, R. M. AGRAWAL, X-Ray Spectrom., 16 (1986) 23.

    Article  Google Scholar 

  13. B. W. BUDESINSKY, X-Ray Spectrom., 9 (1980) 13.

    Article  Google Scholar 

  14. R. A. SMITH, Adv. X-Ray Anal., 25 (1982) 103.

    Google Scholar 

  15. K. C. STEHR, Adv. X-Ray Anal., 25 (1982) 173.

    Google Scholar 

  16. E. P. BERTIN, Principles and Practice of X-Ray Spectrometric Analysis, Plenum Press, New York, 1975.

    Google Scholar 

  17. J. G. DICK, C. C. WAN, R. DIFRUSCIA, X-Ray Spectrom., 6 (1977) 212.

    Article  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Rights and permissions

Reprints and permissions

About this article

Cite this article

Khatri, R.P. Effect of helium environment and mylar foil on the sensitivity of different elements in energy dispersive X-ray fluorescence spectroscopy. Journal of Radioanalytical and Nuclear Chemistry, Articles 134, 53–63 (1989). https://doi.org/10.1007/BF02047270

Download citation

  • Received:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF02047270

Keywords

Navigation