Abstract
A simple method is described for use with the differential scanning calorimeter for baseline interpolation in continual processes over a wide temperature interval. For the process of water desorption from the synthetic zeolite LiA with the coveragegq=1.5, the measured heat of desorption wasQ=11.2±0.5 kcal/mole.
References
L. G. Berg andV. P. Egunov, J. Thermal Anal., 1 (1969) 5.
S. L. Boersma, J. Am. Ceram. Soc., 38 (1955) 281.
M. J. Vold, Anal. Chem., 21 (1949) 683.
P. Murray andJ. White, Trans. Brit. Ceram. Soc., 48 (1949) 187.
H. E. Kissinger, Anal. Chem., 29 (1957) 1702.
F. W. Wilburn, J. Soc. Glass Technol, 38 (1954) 371 T.
F. W. Wilburn, J. R. Hesford andJ. R. Flower, Anal. Chem., 40 (1968) 777.
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The authors wish to thank V. Vučelić and D. Karaulić for their help and interest in solving the problem of the baseline interpolation.
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Vučelić, D., Stamatović, A. & Todorić, U. Baseline interpolation in DTA and DSC quantitative analysis of slow processes. Journal of Thermal Analysis 4, 479–482 (1972). https://doi.org/10.1007/BF01913806
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DOI: https://doi.org/10.1007/BF01913806