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A method for the determination of lattice parameters on single crystals

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Czechoslovak Journal of Physics B Aims and scope

Abstract

The ratio method, designed originally for powder materials, is modified for single crystals. A relatively simple goniometer with photographic registration is used. Discussion of random and systematic errors shows that an accuracyΔa/a = 10−4, or better, can be achieved. An application for single crystals of Fe and Fe-Si alloys is demonstrated. For pure iron the valuea= = (2·8664±00001)×10−10 m is found.

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Authors and Affiliations

  1. Institute of Physics, Czechosl. Acad. Sci., Prague, Na Slovance 2, 180 40, Praha 8, Czechoslovakia

    M. Polcarová & J. Zůra

Authors
  1. M. Polcarová
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  2. J. Zůra
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Polcarová, M., Zůra, J. A method for the determination of lattice parameters on single crystals. Czech J Phys 27, 322–331 (1977). https://doi.org/10.1007/BF01587363

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  • DOI: https://doi.org/10.1007/BF01587363

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