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Crystal and molecular structure ofcis-dibenzobicyclo[3.3.0]octa-2,7-diene, C16H14

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Abstract

The structure of the title compound, C16H14, was determined by X-rays:M r =206.29, monoclinic, space groupP21/n,a=5.002(1),b=23.972(5),c=9.505(2) Å,β=102.56(2)°,V c =1112.4 Å3,Z=4,D x =1.23 Mg m−3, MoKα radiation (graphite crystal monochromator,\(\bar \lambda = 0.71069\) Å),μ(MoKα)=0.75 cm−1,T=290 K. Final conventionalR-factor=0.028,R w =0.030 for 742 unique reflections and 187 variables. The structure was solved usingMultan.

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Authors and Affiliations

  1. Crystallography Laboratory, University of Nijmegen, Toernooiveld, 6525, ED Nijmegen, The Netherlands

    J. M. M. Smits, J. H. Noordik & Paul T. Beurskens

  2. Department of Organic Chemistry, University of Nijmegen, Toernooiveld, 6525, ED Nijmegen, The Netherlands

    W. H. Laarhoven & F. A. T. Lijten

Authors
  1. J. M. M. Smits
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  2. J. H. Noordik
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  3. Paul T. Beurskens
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  4. W. H. Laarhoven
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  5. F. A. T. Lijten
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Smits, J.M.M., Noordik, J.H., Beurskens, P.T. et al. Crystal and molecular structure ofcis-dibenzobicyclo[3.3.0]octa-2,7-diene, C16H14 . Journal of Crystallographic and Spectroscopic Research 16, 23–29 (1986). https://doi.org/10.1007/BF01566043

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  • DOI: https://doi.org/10.1007/BF01566043

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