Abstract
Phosphates of K and Zr of a layered, microporous structure have been obtained by the molten salt method in a potassium nitrate medium in the temperatures range 573–823 K. Dependences of the product composition on the P/Zr atomic ratio and the temperature of synthesis were studied. The substances obtained have been characterized by XRD,1H and31P NMR, and IR spectroscopy, and scanning electron microscopy.
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Translated fromIzvestiya Akademii Nauk. Seriya Khimicheskaya, No. 12, pp. 2847–2851, December, 1996.
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Barabanova, A.V., Afanas'ev, P.V., Kostyuk, B.G. et al. Synthesis of K-Zr phosphates by the molten salt method. Russ Chem Bull 45, 2698–2702 (1996). https://doi.org/10.1007/BF01430625
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DOI: https://doi.org/10.1007/BF01430625