Abstract
The determination of nickel by ETA-AAS and ICP-AES in biological samples with prior extraction into methyl isobutyl ketone with 1,5-bis(di-2-pyridylmethylene) thiocarbonohydrazide as extracting reagent is described. Microwave dissolution in closed teflon vessels has been used for the dissolution of biological materials. At least three samples can be decomposed simultaneously with a preset heating programme. Results of analyses of some certified biological reference materials are given.
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Alonso, E.V., de Torres, A.G. & Cano Pavón, J.M. Determination of nickel in biological samples by ETA-AAS and ICP-AES after acidic dissolution (with microwave heating and preconcentration by liquid-liquid extraction). Mikrochim Acta 110, 41–45 (1993). https://doi.org/10.1007/BF01243983
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DOI: https://doi.org/10.1007/BF01243983