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Development of a method for analyzing volatiles from foodstuff matrices, including microextraction by demixture. Application to the analysis of grapes

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Abstract

This paper presents a general method for analyzing volatiles from foodstuff samples, and its application to the analysis of grapes. The method includes steam stream distillation, microextraction and chromatographic analysis, and all aspects of the analysis, including sample treatment, are discussed. Data on recovery and reproducibility are given. The method allows to prepare samples for quantitative chromatographic analysis in only one hour and to quantitate the volatiles present in the original samples at concentrations between 0.2 and 2000 mg 1−1 with FID detection.

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References

  1. M. M. Leahy, and G. A. Reineccius, in:Analysis of Volatiles (P. Schreier, ed.), W. de Gruyter, New York, 1984, pp. 19–47.

    Google Scholar 

  2. H. Sugisawa, in:Analysis of Volatiles (P. Schreier, ed.), W. de Gruyter, New York, 1984, pp. 3–18.

    Google Scholar 

  3. S. S. Chang, F. M. Vallese, L. S. Hwang, O. Hsieh, D. Min,J. Agric. Food Chem. 1977,25(3), 450.

    Google Scholar 

  4. W. G. Jennings, M. Filsoof,J. Agric. Food Chem. 1977,25(3), 440.

    Google Scholar 

  5. C. Weurman,J. Agric. Food Chem. 1969,17(2), 370.

    Google Scholar 

  6. J. Cache, V. Ferreira,Analyst. 1990,115(5), 657.

    Google Scholar 

  7. J. Cacho, V. Ferreira, (in preparation).

  8. H. Schmidt,Z. Anal. Chem. 1960,178, 173.

    Google Scholar 

  9. K. Grob, K. Grob Jr.,J. HRC & CC 1978,1, 57.

    Google Scholar 

  10. K. Grob,Classical Split and Splitless Injection in Capillary, G. C. Huethig Verlag, 1988.

  11. F. J. Yang, A. C. Brown III, S. P. Cram,J. Chrom. 1978,158, 91.

    Google Scholar 

  12. K. Grob, E. Müller,J. Chrom. 1987,404, 297.

    Google Scholar 

  13. P. J. Hardy,Agric. Food Chem. 1969,17(3), 656.

    Google Scholar 

  14. A. P. Aryan, B. Wilson, C. R. Strauss, P. J. Williams,Am. J. Enol. Vitic. 1987,38(3), 182.

    Google Scholar 

  15. C. Bayonove, Z. Gunata, A. Cordonnier,Bull. OIV. 1988,643, 741.

    Google Scholar 

  16. F. Drawert, R. Tressl, W. Hermann, R. Emberger, M. Speck,Chem. Mikrobiol. Technol. Lebensm. 1973,2, 10.

    Google Scholar 

  17. W. H. Wolfe,Am. J. Enol. Vitic. 1976,27, 68.

    Google Scholar 

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Authors and Affiliations

  1. Department of Analytical Chemistry, Sciences Faculty, University of Zaragoza, E-50009, Zaragoza, Spain

    Juan Cacho, Javier Melendez & Vicente Ferreira

Authors
  1. Juan Cacho
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  2. Javier Melendez
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  3. Vicente Ferreira
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Cacho, J., Melendez, J. & Ferreira, V. Development of a method for analyzing volatiles from foodstuff matrices, including microextraction by demixture. Application to the analysis of grapes. Mikrochim Acta 108, 61–72 (1992). https://doi.org/10.1007/BF01240372

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  • DOI: https://doi.org/10.1007/BF01240372

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