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Microanalysis of CH3-bearing functional groups by nuclear magnetic resonance spectrometry

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Summary

A method is described for the quantitative microanalysis of C-CH3, 0-CH3, -COCH3, N-CH3, and S-CH3 functions by NMR spectrometry. From 4 to 11 mg of the organic compound is used for a determination.

Zusammenfassung

Eine quantitative Mikromethode zur Bestimmung von C-Methyl, Methoxyl, Acetyl, N-Methyl und Thiomethyl mit Hilfe der Kernresonanz-Spektrometrie wurde beschrieben. 4 bis 11 mg Substanz werden für eine Bestimmung verwendet.

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References

  1. C. A. Reilly, Analyt. Chemistry30, 839 (1958).

    Google Scholar 

  2. P. W. Flanagan andH. F. Smith, Analyt. Chemistry34, 699 (1962).

    Google Scholar 

  3. H. Y. Chen, Analyt. Chemistry34, 793 (1962).

    Google Scholar 

  4. P. W. Flanagan, R. A. Greff, andH. F. Smith, Analyt. Chemistry35, 1283 (1963).

    Google Scholar 

  5. H. F. White, C. W. Davisson, andV. A. Yarborough, Analyt. Chemistry36, 1659 (1964).

    Google Scholar 

  6. C. A. Glass andH. J. Dutton, Analyt. Chemistry38, 472 (1966).

    Google Scholar 

  7. A. Mathias andN. Mellor, Analyt. Chemistry38, 472 (1966).

    Google Scholar 

  8. N. v. Meurs, Z. analyt. Chem.205, 194 (1964).

    Google Scholar 

  9. T. F. Page, jr., andW. E. Bresler, Analyt. Chemistry36, 1981 (1964).

    Google Scholar 

  10. M. W. Dietrich, J. S. Nash, andR. E. Keller, Analyt. Chemistry38, 1479 (1966).

    Google Scholar 

  11. L. P. Lindeman andS. W. Nicksic, Analyt. Chemistry36, 2414 (1964).

    Google Scholar 

  12. J. C. N. Ma andE. W. Warnhoff, Can. J. Chem.43, 1849 (1965).

    Google Scholar 

  13. R. J. Day andC. N. Reilley, Analyt. Chemistry38, 1323 (1966).

    Google Scholar 

  14. M. W. Dietrich andR. O. Keller, Analyt. Chemistry36, 2174 (1964).

    Google Scholar 

  15. R. J. Kula, D. L. Rabenstein, andG. H. Reed, Analyt. Chemistry35, 1783 (1963).

    Google Scholar 

  16. J. L. Jungnickel andJ. W. Forbes, Analyt. Chemistry35, 938 (1936).

    Google Scholar 

  17. P. J. Paulsen andW. D. Cooke, Analyt. Chemistry36, 1713 (1964).

    Google Scholar 

  18. P. J. Paulsen andW. D. Cooke, Analyt. Chemistry36, 1721 (1964).

    Google Scholar 

  19. F. F. Caserio, Analyt. Chemistry38, 1802 (1966).

    Google Scholar 

  20. K. G. Stone, inI. M. Kolthoff andP. J. Elving (eds.), Treatise on Analytical Chemistry, part II, section B, vol. 13. New York: Wiley. 1966.

    Google Scholar 

  21. N. D. Cheronis andT. S. Ma, Organic Functional Group Analysis by Micro and Semimicro Methods. New York: Wiley. 1964.

    Google Scholar 

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Authors and Affiliations

  1. Department of Chemistry, University of Maryland, 20740, College Park, Md., USA

    F. Kasler

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  1. F. Kasler
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Kasler, F. Microanalysis of CH3-bearing functional groups by nuclear magnetic resonance spectrometry. Mikrochim Acta 55, 1065–1076 (1967). https://doi.org/10.1007/BF01225944

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  • DOI: https://doi.org/10.1007/BF01225944

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