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Micro determination of olefinic unsaturation using bromine monochloride in acetic acid medium

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Summary

A micro procedure for the determination of olefinic unsaturation in organic compounds using bromine monochloride in acetic acid as the reagent is described. The results obtained show a maximum deviation of about 1.5% C=C in most cases.

Zusammenfassung

Ein Mikroverfahren zur Bestimmung von C=C-Bindungen mit Brommonochlorid in Essigsäurelösung wurde beschrieben. Die maximale Abweichung beträgt meist 1,5%.

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Authors and Affiliations

  1. Department of Chemistry, University of Allahabad, Allahabad, India

    J. P. Sharma, A. K. Awasthy & V. K. S. Shukla

Authors
  1. J. P. Sharma
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  2. A. K. Awasthy
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  3. V. K. S. Shukla
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Sharma, J.P., Awasthy, A.K. & Shukla, V.K.S. Micro determination of olefinic unsaturation using bromine monochloride in acetic acid medium. Mikrochim Acta 60, 522–525 (1972). https://doi.org/10.1007/BF01217958

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  • DOI: https://doi.org/10.1007/BF01217958

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