Skip to main content
Log in

Beitrag zur Kenntnis der Methoxyl- und Methylimidbestimmung

Contribution to the knowledge of the determination of methoxyl and methylimide

  • Published:
Microchimica Acta Aims and scope Submit manuscript

Zusammenfassung

Ein neues verbessertes Gerät wird beschrieben, das sich für Methoxylund Methylimidbestimmungen, speziell in der gravimetrischen Ausführung nachMitsui eignet. Außerdem werden Beobachtungen zu einigen Details solcher Bestimmungen, der Wirkung phosphorhaltiger Reduktionsmittel, Ammoniumjodid und Phenol, mitgeteilt. ab]Summary

A new improved device is described, which is suitable for the determinations of methoxyl and methylimide, especially in the gravimetric determination afterMitsui. In addition, observations are reported regarding several details of such determinations, the action of phosphorus-bearing reducing agent, ammonium iodide and phenol.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Literatur

  1. R. Belcher, Submicro Methods of Organic Analysis. Amsterdam: Elsevier. 1966.

    Google Scholar 

  2. L. Filipovic undZ. Stefanac, Croat. Chim. Acta30, 149 (1958).

    Google Scholar 

  3. F. Franzen, K. Eysell undH. Schall, Mikrochim. Acta [Wien]1954, 712.

  4. F. Franzen undH. Pauli, Mikrochim. Acta [Wien]1955, 845.

  5. F. Friedrich, Mikrochem.7, 185 (1929).

    Google Scholar 

  6. M. Fukuda, Mikrochim. Acta [Wien]1960, 448.

  7. J. Herzig undJ. Meyer, Ber. dtsch. chem. Ges.27, 319 (1894).

    Google Scholar 

  8. J. Herzig undJ. Meyer, Mh. Chem.15, 613 (1894).

    Google Scholar 

  9. A. S. Inglis, Mikrochim. Acta [Wien]1957, 677.

  10. W. Kirsten undS. Ehrlich-Rogozinsky, Mikrochim. Acta [Wien]1955, 786.

  11. T. Mitsui, Microchem. J., Symp. Ser.2, 571 (1961).

    Google Scholar 

  12. T. Mitsui undY. Kitamura, Microchem. J.7, 141 (1963).

    Google Scholar 

  13. M. M. Sohachter undT. S. Ma, Mikrochim. Acta [Wien]1966, 55.

  14. A. A. Sirotenko, Mikrochim. Acta [Wien]1955,1.

  15. H. Swift, unveröffentlicht durchS. J. Clark „Quantitative Methods of Organic Microanalysis”. London: Butterworth. 1956.

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Rights and permissions

Reprints and permissions

About this article

Cite this article

Trutnovsky, H., Sakla, A.B. & Haller, P. Beitrag zur Kenntnis der Methoxyl- und Methylimidbestimmung. Mikrochim Acta 58, 1277–1282 (1970). https://doi.org/10.1007/BF01215966

Download citation

  • Received:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF01215966

Navigation