Summary
The 3,5-dinitrobenzoates of alcohols can easily be prepared on a small scale by first forming the sodium alcoholates by the use of a sodium dispersion.
Zusammenfassung
Alkohol-3,5-dinitrobenzoate lassen sich in kleinem Maßstab leicht herstellen, indem man mit Hilfe einer Natriumdispersion zunächst das betreffende Natriumalkoholat bildet.
Résumé
On peut préparer facilement et sur une petite échelle, les dinitro-3,5-benzoates d'alcools en formant d'abord les alcoolates de sodium à l'aide de sodium dispersé.
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References
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R. E. Dunbar andF. J. Ferrin, Chemist-Analyst44, 77 (1955).
I. Fatt andM. Tashima, Alkali Metal Dispersions. Princeton, N. J.: Van Nostrand. 1961. pp. 78–79.
J. Patrick andF. Schneider, Mikrochim. Acta [Wien]1960, 970.
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Kunzer, A.H., Schneider, F.L. Sodium dispersions in the preparation of 3,5-dinitrobenzoates of alcohols. Mikrochim Acta 52, 25–27 (1964). https://doi.org/10.1007/BF01215660
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DOI: https://doi.org/10.1007/BF01215660