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Micro determination of active hydrogen in organic compounds by lithium-aluminum hydride

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Summary

Roth's apparatus for the micro determination of active hydrogen according toZerewitinoff has been used to quantitatively estimate active hydrogen with the use of lithium-aluminum hydride. A suitable procedure has been evolved.

Zusammenfassung

DieRothsche Apparatur für die Mikrobestimmung nachZerewitinoff wird für die Bestimmung des aktiven Wasserstoffes mit Lithiumaluminiumhydrid verwendet. Dadurch wird der störende Einfluß von im Lösungsmittel und im Apparat etwa vorhandenen Feuchtigkeitsspuren vermieden.

Résumé

L'appareil deRoth pour le microdosage de l'hydrogène actif en accord avecZerewitinoff, a été utilisé pour doser quantitativement l'hydrogène actif par emploi de l'hydrure de lithium-aluminium. Un procédé convenable a été mis au point.

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Authors and Affiliations

  1. National Chemical Laboratory of India, Poona 8, India

    D. Subba Kao, G. D. Shah & V. S. Pansare

Authors
  1. D. Subba Kao
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  2. G. D. Shah
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  3. V. S. Pansare
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Subba Kao, D., Shah, G.D. & Pansare, V.S. Micro determination of active hydrogen in organic compounds by lithium-aluminum hydride. Mikrochim Acta 42, 81–84 (1954). https://doi.org/10.1007/BF01215573

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  • DOI: https://doi.org/10.1007/BF01215573

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