Skip to main content
SpringerLink
Log in

Extraction chromatography preconcentration of impurities from high purity lead

  • Published:
Microchimica Acta Aims and scope Submit manuscript

Summary

The method of multielement preconcentration of impurities from high-purity lead utilizing an extraction Chromatographie separation in tri-n-octylamine-HCl system is developed. Unlike a well-known procedure based on precipitation of lead nitrate this method is applicable to very small samples. Being used in combination with the precipitation procedure mentioned, this method provides a considerable increase in the effectiveness of the latter.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

References

  1. R. G. Pearson, J. Chem. Educ.45, 581 (1968).

    Google Scholar 

  2. J. A. Corbett, Metallurgia65, 43 (1962).

    Google Scholar 

  3. H. Jedrzejewska and M. Malusecka, Chem. Anal. (Warsaw)12, 579 (1967).

    Google Scholar 

  4. T. Yamane, T. Mukoyama, and T. Sasamoto, Anal. Chim. Acta69, 347 (1974).

    Google Scholar 

  5. M. Hiraide and A. Mizuike, Talanta22, 539 (1975).

    Google Scholar 

  6. K. Lorber and K. Müller, Mikrochim. Acta [Wien]1976 I, 375.

    Google Scholar 

  7. E. Jackwerth, Pure Appl. Chem.51, 1149 (1979).

    Google Scholar 

  8. T. Brown and G. Ghersini (eds.), Extraction Chromatography, Budapest: Akadémiai Kiadó and Amsterdam: Elsevier 1975. p. 565.

    Google Scholar 

  9. S. S. Grazhulene, S. A. Poluyanova, O. I. Kharitonova, and Yu. I. Popandopulo, Mikrochim. Acta [Wien]1982 II, 231.

    Google Scholar 

  10. S. S. Grazhulene, V. K. Karandashev, Yu. I. Popandopulo, N. I. Chaplygina, and Yu. V. Yakovlev, Mikrochim. Acta [Wien]1984 II, 301.

    Google Scholar 

  11. T. Ishimori, E. Akatsu, R. Tsukuechi, T. Kobune, J. Usuba, K. Kimura, G. Onawa, and H. Uchiyama, Rept. JAERI-1106, 1966.

Download references

Author information

Authors and Affiliations

  1. Institute of Problems of Microelectronics Technology and Superpure Materials, U. S. S. R. Academy of Sciences, Chernogolovka, Moscow District, USSR

    S. S. Grazhulene, V. Yu. Nagy, T. A. Orlova, V. V. Kireiko & G. F. Telegin

Authors
  1. S. S. Grazhulene
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. V. Yu. Nagy
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. T. A. Orlova
    View author publications

    You can also search for this author in PubMed Google Scholar

  4. V. V. Kireiko
    View author publications

    You can also search for this author in PubMed Google Scholar

  5. G. F. Telegin
    View author publications

    You can also search for this author in PubMed Google Scholar

Rights and permissions

Reprints and permissions

About this article

Cite this article

Grazhulene, S.S., Nagy, V.Y., Orlova, T.A. et al. Extraction chromatography preconcentration of impurities from high purity lead. Mikrochim Acta 86, 153–160 (1985). https://doi.org/10.1007/BF01197814

Download citation

  • Received:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF01197814

Keywords

Search

Navigation