Skip to main content
SpringerLink
Log in

Determination of thioacetamide with ceric sulphate, sodium vanadate, manganese (III), and potassium ferricyanide

  • Published:
Microchimica Acta Aims and scope Submit manuscript

Summary

The determination of thioacetamide in sulphuric acid medium with ceric sulphate, sodium vanadate, manganese (III) and potassium ferricyanide is described. A mixture of potassium iodate and potassium iodide (iodine) is used as the catalyst to accelerate the reaction. Ferroin is used as the indicator.

Zusammenfassung

Die Bestimmung von Thioacetamid in schwefelsaurem Milieu mit Cer(IV)sulfat, Natriumvanadat, Mangan(III) und Kaliumcyanoferrat(III) wurde beschrieben. Eine Mischung aus Kaliumjodat und -jodid dient als Katalysator zur Beschleunigung der Reaktion. Ferroin wird als Indikator verwendet.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

References

  1. H. Flaschka, Chemist Analyst44, 2 (1955).

    Google Scholar 

  2. S. Y. Shen and M. Kakaty, Mikrochim. Acta [Wien]1971, 96.

  3. E. H. Swift and F. C. Anson, in C. N. Reily (Ed.): Advances in Analytical Chemistry and Instrumentation, Volume-I, New York: Interscience. 1960. p. 293.

    Google Scholar 

  4. A. Milczarska and S. Petri, Ann. acad. med. Lodz8, 157 (1966).

    Google Scholar 

  5. A. Claeys, H. Sion, A. Campe, and H. Thun, Bull. soc. chim. Belge70, 576 (1961).

    Google Scholar 

  6. T. J. Jacob and C. G. R. Nair, Talanta13, 154 (1966).

    Google Scholar 

  7. M. Sarwar and R. J. Thibert, Anal. Lett.116, 381 (1968).

    Google Scholar 

  8. C. G. R. Nair, (Miss) S. Geatha, and P. T. Joseph, Indian J. Appl. Chem.30, 60 (1967).

    Google Scholar 

  9. R. J. Thibert and M. Sarwar, Microchem. J.14, 27 (1969).

    Google Scholar 

  10. M. K. Papay, R. Toth, V. Izvekov, and E. Pungor, Analyt. Chim. Acta64, 409 (1973).

    Google Scholar 

  11. M. Pryszczewska and E. Krzezowska, Zeszyty Nauk. Polytech. Szezecin. Chim.6, 15 (1965).

    Google Scholar 

  12. D. M. King and W. S. Eton, Talanta15, 347 (1968).

    Google Scholar 

  13. M. Pryszczewska, Talanta13, 1700 (1966).

    Google Scholar 

  14. K. Lesz, H. Wieczorkiewicz, and J. Lipiec, Chem. Anal. (Warsaw)6, 1033 (1961).

    Google Scholar 

  15. S. Washizuka, Bunseki Kagaku16, 963 (1967).

    Google Scholar 

  16. I. M. Kolthoff, R. Belcher, V. A. Stenger, and G. Matsuana, Volumetric analysis (III), New York: Interscience. 1957. p. 128, 237 and 634.

    Google Scholar 

  17. C. O. Ingamells, Talanta2, 171 (1959).

    Google Scholar 

  18. A. Berka, J. Vulterin, and J. Zyka, Newer Redox Titrants, London: Pergamon. 1965. p. 11.

    Google Scholar 

  19. G. Gopala Rao, M. Gandikota, and S. G. Viswanath, Analyt. Chim. Acta87, 511 (1976).

    Google Scholar 

Download references

Author information

Authors and Affiliations

  1. Department of Chemistry, Analytical Branch, Jeypore Vikrama Deo College of Science and Technology, Andhra University, 530003, Waltair, India

    N. Krishna Murty, G. Upendra Prasad & K. Rama Rao

Authors
  1. N. Krishna Murty
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. G. Upendra Prasad
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. K. Rama Rao
    View author publications

    You can also search for this author in PubMed Google Scholar

Rights and permissions

Reprints and permissions

About this article

Cite this article

Krishna Murty, N., Upendra Prasad, G. & Rama Rao, K. Determination of thioacetamide with ceric sulphate, sodium vanadate, manganese (III), and potassium ferricyanide. Mikrochim Acta 70, 89–94 (1978). https://doi.org/10.1007/BF01196471

Download citation

  • Received:

  • Revised:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF01196471

Keywords

Search

Navigation