Summary
The 4-heptanone oxime extraction procedure may be used for the quantitative separation of trace amounts of palladium from a noble-metals-bearing sulfide concentrate. An average palladium value of 0.335 oz/ton was obtained on a standard sample compared to the recommended value of 0.37 oz/ton.
Zusammenfassung
Für die quantitative Abtrennung von Palladiumspuren aus einem edelmetallhaltigen Sulfidkonzentrat eignet sich die Extraktion mit 4-Heptanonoxim. In einer Standardprobe, deren Palladiumgehalt mit 0,37 Unzen/Tonne angegeben war, wurden durchschnittlich 0,335 Unzen/Tonne gefunden.
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References
R. J. Walker and W. J. Holland, Mikrochim. Acta [Wien]1975 II, 541.
W. J. Holland, R. A. Dimenna and R. J. Walker, Mikrochim. Acta [Wien]1972, 183.
R. C. McAdam, Sutarno and P. E. Moloughney, “Noble-Metals-Bearing Sulfide Concentrate PTC: Its Characterization and Preparation for Use as a Standard Reference Material”. Department of Energy, Mines and Resources, Mines Branch, Ottawa. Technical Bulletin TB 176,1973.
R. J. Walker and W. J. Holland, Mikrochim. Acta [Wien]1973, 591.
W. J. Holland and J. Bozic, Analyt. Chemistry40, 433 (1968).
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Dupuis, L.T., Holland, W.J. Alkyl ketoximes as analytical reagents. XI. Mikrochim Acta 67, 483–487 (1977). https://doi.org/10.1007/BF01195959
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DOI: https://doi.org/10.1007/BF01195959