Abstract
The title compound (C19H18O2N2Cl2) crystallized in the monoclinic space groupP21/n witha=13.062(2),b=10.931(2),c=13.120(2)Å, andβ=104.57(1)°. The structure was solved by direct methods and refined toR=0.047 for 2776 reflections. The piperidine ring assumes a distorted boat conformation. The angle between phenyl rings is 78.98(7)°. The nitroso group is oriented by 138.22(7)° to the best plane of the piperidine ring. The interaction between the molecules are van der Waals in nature.
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Sukumar, N., Ponnuswamy, M.N., Thenmozhiyal, J.C. et al. Crystal and molecular structure of 2,6-di (o-chloro)phenyl-3,5-dimethyl-N-nitrosopiperidin-4-one(NOCDMPO). Journal of Crystallographic and Spectroscopic Research 23, 871–875 (1993). https://doi.org/10.1007/BF01195734
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DOI: https://doi.org/10.1007/BF01195734