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Crystal and molecular structure of 6-chloro-3-cyclopentylmethyl-3,4-dihydro-7-sulfamyl-2H-1,2,4-benzothiadiazine-1,1-dioxide

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Abstract

The crystal structure of the title compound, C13H18N3O4S2C1, a sulfa drug, has been determined by X-ray diffraction data using MoKα radiation. The crystals are orthorhombic,Pbca, witha=9.441(4),b=29.633(11),c=12.167(8) Å andZ=8. The structure was solved by the heavy-atom method, and refined by full matrix least-squares to a finalR value of 0.054 with 2062 observed reflections. In the crystal, the molecules are linked by N-H⋯O hydrogen bonds.

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Authors and Affiliations

  1. Crystallography and Molecular Biology Division, Saha Institute of Nuclear Physics, Sector I, Block AF Bidhannagar, 700 064, Calcutta, India

    A. K. Basak, M. Ghosh & S. K. Mazumdar

  2. Bose Institute, 93/1 Acharya Prafulla Chandra Road, 700 009, Calcutta, India

    S. Chaudhuri

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  1. A. K. Basak
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  2. M. Ghosh
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  3. S. K. Mazumdar
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  4. S. Chaudhuri
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Basak, A.K., Ghosh, M., Mazumdar, S.K. et al. Crystal and molecular structure of 6-chloro-3-cyclopentylmethyl-3,4-dihydro-7-sulfamyl-2H-1,2,4-benzothiadiazine-1,1-dioxide. Journal of Crystallographic and Spectroscopic Research 19, 547–560 (1989). https://doi.org/10.1007/BF01185390

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  • DOI: https://doi.org/10.1007/BF01185390

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