Skip to main content
SpringerLink
Log in

Crystal structure and spectroscopic study of 2-(p-methoxycarbonylphenyl)-1,3,5,5,7,8,8-heptamethyl-2,4,5,6,7,8-hexahydroindeno[1,2-c]-pyrrole-7-carbonitrile

  • Published:
Journal of Crystallographic and Spectroscopic Research Aims and scope Submit manuscript

Abstract

The crystal structure of the title compound has been determined. The crystals are orthorhombic:Pbnb, (bca setting of Pccn, No 56),a=18.053(8),b=15.532(4),c=16.915(6) Å,V c =4743(3) Å3,Z=8,D x =1.17 Mg m−3,λ=(MoKα)=0.71069 Å. The structure was solved by direct methods and refined with 1352 reflections to a finalR value of 0.067. Mass and spectral data (IR, UV,1H and13C NMR) are also reported.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

References

  • Camps F., Coll, J., Mola, C., and Muñoz, F. (1985) Comunicación a la XI Reunión Bienal de Química Organica. (R. S. E. Q.).

  • Duax, W. L., and Norton, D. A. (1975)Atlas of Steroid Structure (Plenum Press, New York, London).

    Google Scholar 

  • Gollmick, K., Shade, G., Cameron, A. F., Hannaway, C., Roberts, J. S., and Roberston, J. M. (1970)J. Chem. Soc. D 248–249.

  • International Tables for X-Ray Crystallography. (1974) Vol. IV, Kynoch Press, Birmingham (Present Distributor D. Reidel, Dordrecht), pp. 99, 149.

  • Krivenko, A. P., Nikolaeva, T. G., Espenbetov, A. A., Komyagin, N. T., Sorokin, N. N., Struchkov, Yu. T., and Karchenko, V. G. (1985)Khim. Geterotsikl. Soedin., 71–75.

  • Main, P., Germain, G., and Woolfson, M. M., (1984)Multan 11/84. A system of computer programs for the automatic solution of crystal structures from X-ray diffraction data. (Univ. of York, England, and Louvain, Belgium).

    Google Scholar 

  • Motherwell, W. D. S., and Clegg, W. (1978)Pluto78. Program for plotting molecular and crystal structures. (Univ. of Cambridge, England).

    Google Scholar 

  • Oesterlin, R., Bell, M. R., McGarry, R. H., Hlavac, A. G., Bradford, J. C., and Rozitis, J., Jr. (1977)J. Med. Chem. 20, 1068–1071.

    Google Scholar 

  • Sheldrick, G. M. (1976)Shelx 76. Program for crystal structure determination. (Univ. of Cambridge, England).

    Google Scholar 

Download references

Author information

Authors and Affiliations

  1. Departamento de Química Orgánica Biológica C. I. D. (CSIC), Jordi Girona, 18, 08034, Barcelona, Spain

    F. Camps, J. Coll & C. Mola

  2. Institut de Ciència de Materials de Barcelona (CSIC), Martí i Franqués, s/n. Apartado de Correos 30102, 08028, Barcelona, Spain

    J. Rius, E. Molins & C. Miravitlles

Authors
  1. F. Camps
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. J. Coll
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. C. Mola
    View author publications

    You can also search for this author in PubMed Google Scholar

  4. J. Rius
    View author publications

    You can also search for this author in PubMed Google Scholar

  5. E. Molins
    View author publications

    You can also search for this author in PubMed Google Scholar

  6. C. Miravitlles
    View author publications

    You can also search for this author in PubMed Google Scholar

Rights and permissions

Reprints and permissions

About this article

Cite this article

Camps, F., Coll, J., Mola, C. et al. Crystal structure and spectroscopic study of 2-(p-methoxycarbonylphenyl)-1,3,5,5,7,8,8-heptamethyl-2,4,5,6,7,8-hexahydroindeno[1,2-c]-pyrrole-7-carbonitrile. Journal of Crystallographic and Spectroscopic Research 19, 873–882 (1989). https://doi.org/10.1007/BF01185353

Download citation

  • Received:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF01185353

Keywords

Search

Navigation