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Derivatives of unsaturated phosphonic acids

communication 13. Diesters of 2-(2-alkoxyethoxy)vinylphosphono-mono-,di-, and-trithionic acids

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Bulletin of the Academy of Sciences of the USSR, Division of chemical science Aims and scope

Summary

  1. 1.

    Reaction of 2-(2-alkoxyethoxy) vinylphosphonothioic dichlorides with sodium methoxide and ethoxide yielded 0.0-dimethyl and 0.0-diethyl esters of 2-(2-methoxyethoxy)-, 2-(2-ethoxyethoxy)- and 2-(2-butoxy-ethoxy)-vinylphosphenothioic acids.

  2. 2.

    Reaction of 2-(2-alkoxyethoxy)vinylphosphonic and 2-(2-alkoxyethoxy)vinylphosphonothioic dichlorides with sodium ethylmercaptide yielded S,S-diethyl 2-(2-methoxyethoxy)- and 2-(2-butoxyethoxy)-vinylphophonothioares and diethyl 2-(2-methoxyethoxy)- and 2-(3-ethoxyethoxy)-vinylphosphonotrithioates.

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Literature cited

  1. K. N. Anisimov, N. E. Kolobova and A. N. Nesmeyanov, Bull. Acad. Sci., USSR, Div. Chem. Sci., 1954, No. 9, 799 (T. p. 689).

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Authors and Affiliations

  1. Institute of Heteroorganic Compounds of the USSR Academy of Sciences, Germany

    K. N. Anisimov, N. E. Kolobova & A. N. Nesmeyanov

Authors
  1. K. N. Anisimov
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  2. N. E. Kolobova
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  3. A. N. Nesmeyanov
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Anisimov, K.N., Kolobova, N.E. & Nesmeyanov, A.N. Derivatives of unsaturated phosphonic acids. Russ Chem Bull 4, 911–913 (1955). https://doi.org/10.1007/BF01172108

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  • DOI: https://doi.org/10.1007/BF01172108

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