Summary
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1.
Lithium aluminum hydride has been prepared in bis-(2-ethoxyethyl) ether.
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2.
A method has been devised for the micro synthesis and isolation of methanol labeled with radiocarbon.
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3.
Ethanol labeled with radiocarbon in the CH3 group has been synthesized for the first time.
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4.
A method has been devised for the micro synthesis of labeled ethyl acetate from barium acetate.
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5.
A method has been devised for the micro synthesis and isolation of ethanol labeled with radiocarbon in the 1-position.
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6.
Two isotopic isomers of acetaldehyde have been prepared.
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Feklisov, G.I. Application of lithium aluminum hydride in micro syntheses with labeled carbon. Russ Chem Bull 2, 527–534 (1953). https://doi.org/10.1007/BF01171771
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DOI: https://doi.org/10.1007/BF01171771