Skip to main content
SpringerLink
Log in

Method for the preparative of piperazinedione-2,6

  • Published:
Chemistry of Heterocyclic Compounds Aims and scope

Abstract

A method has been developed for the preaparation of piperazinedione-2.6. It consists in the cyclization of iminodiacetic acid with ammonium formate. The dependance of the yield of the final product on the reaction temperature, the ratio of the components, and the choice of the solvent has been investigated.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

References

  1. S. R. Safir and J. J. Hlavka, US Patent 2,762,804; Chem Abstr.,51, 5130c (1957).

    Google Scholar 

  2. M. P. Tneil, French Patent M2392; Chem. Abstr.,61, 8323q (1964).

    Google Scholar 

  3. C. Lavielle and J.-C. Poignaut, French Patent 86-09977; Ref. Zh. Khim., 20094P (1989).

  4. A. M. Greighton, K. Hellmann, and S. Whitecross, Nature222, 384 (1969).

    PubMed  Google Scholar 

  5. I. Saikawa, S. Takano, O. Takashima, K. Momonoi, T. Yasuda, K. Kasuya, and M. Kamatsu, J. Pharm. Soc. Jpn.,97, 980 (1977).

    Google Scholar 

  6. M. A. Weaver and D. J. Wallace, Belgian Patent 669062; Chem. Abstrs.,65, 9061 h (1966).

    Google Scholar 

  7. R. Epton, G. Marr, and A. T. Shackley, Polymers,23, 771 (1982).

    Google Scholar 

  8. F. Tieh-Yin and R. Winter, EP Patent 63544; Chem. Abstr.,98, 14498 q (1983)

    Google Scholar 

  9. J. A. Jongkees, Rec. Trav. Chim.,27, 287 (1908).

    Google Scholar 

  10. T. W. H. Cheeseman and E. S. G. Torzs, J. Chem. Soc., No. 12, 6681 (1965).

  11. T. Tanaka, M. Komuro, and M. Ohta, J. Synth. Org. Chem. Jpn.34, 425 RZhKh, 8Zh257 (1977).

    Google Scholar 

  12. B. H. Chase and A. M. Downes, J. Chem. Soc., No. 12, 3974 (1953).

Download references

Author information

Authors and Affiliations

  1. Institute of Biochemistry, 2021, Vilna, Lithuania

    I. P. Shvedaite

Authors
  1. I. P. Shvedaite
    View author publications

    You can also search for this author in PubMed Google Scholar

Additional information

Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 1, pp. 73–75, January, 1995.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Shvedaite, I.P. Method for the preparative of piperazinedione-2,6. Chem Heterocycl Compd 31, 63–65 (1995). https://doi.org/10.1007/BF01171293

Download citation

  • Received:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF01171293

Keywords

Search

Navigation