Abstract
C20H22O4,M r =326.39, triclinic,P¯1,a=10.365(2),b=11.383(2),c=8.461(1) Å, α=103.60(1),β=104.44(1), γ=105.23(1)°,Z=2, λ(CuKα)=1.54178 Å;R=0.0633 for 1940 reflections. The results of the X-ray analysis have shown that the ethyl carboxylate substituent isβ oriented. The geometry of the main skeleton of the molecule has not revealed any significant differences in the present compound and in the case of the epimeric molecule.
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Wieczorek, M. W., Karolak-Wojciechowska, J., and Bujacz, G. D. (1988)J. Crystallogr. Spectrosc. Res. 18, 555.
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Kwiatkowski, W., Karolak-Wojciechowska, J. & Wieczorek, M.W. Crystal and molecular structure of 3-methoxy-6-nor-6,7-secooestra-1,3,5(10),9(11), 14-penten-17-one-8β-ethyl carboxylate. Journal of Crystallographic and Spectroscopic Research 18, 517–523 (1988). https://doi.org/10.1007/BF01161144
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DOI: https://doi.org/10.1007/BF01161144