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A13C and15N NMR study of some furoxans and related compounds

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Abstract

Carbon and nitrogen NMR results are reported for a collection of furoxans and related compounds, taken on DMSO solutions. The15N chemical shifts and those of neighboring13C nuclei have characteristic values for the structures studied. Relative14N signal widths are used to identify the nitro group resonances. Valence tautomerism at room temperature is reported for one compound. The INADEQUATE technique is used to determine some1J(13C-13C) data.

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Authors and Affiliations

  1. Institute of Organic Chemistry, Polish Academy of Sciences, 01-224, Warsaw, Poland

    B. Kamienski, W. Schilf, J. Sitkowski & L. Stefaniak

  2. Department of Chemistry, University of Surrey, Guildford, GU2 5XH, Surrey, UK

    G. A. Webb

Authors
  1. B. Kamienski
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  2. W. Schilf
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  3. J. Sitkowski
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  4. L. Stefaniak
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  5. G. A. Webb
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Kamienski, B., Schilf, W., Sitkowski, J. et al. A13C and15N NMR study of some furoxans and related compounds. Journal of Crystallographic and Spectroscopic Research 19, 1003–1008 (1989). https://doi.org/10.1007/BF01160882

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  • DOI: https://doi.org/10.1007/BF01160882

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