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Structural and spectroscopic properties of 2-thiophenecarboxaldehyde 2-thienylhydrazone

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Abstract

In this paper the crystal and molecular structure of the title compound is reported. The crystals are monoclinic, P21/c,Z=4,a=13.406(4),b=5.367(1),c=15.545(6)Å,β=110.00(5)°. The structure was solved by direct and Fourier methods and refined by full-matrix least squares toR=0.0497 andRw=0.0537 for 1094 unique reflections. The molecule shows an E-conflguration with respect to the C=N double bond. Mass and IR spectra are also discussed.

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Authors and Affiliations

  1. Istituto di Chimica Generale ed Inorganica Centro di Studio per la Strutturistica Diffrattometrica del C.N.R., University of Parma, Viale delle Scienze, 43100-I, Parma, Italy

    L. P. Battaglia, A. Bonamartini Corradi, G. Pelosi & P. Tarasconi

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  1. L. P. Battaglia
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  2. A. Bonamartini Corradi
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  3. G. Pelosi
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  4. P. Tarasconi
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Battaglia, L.P., Corradi, A.B., Pelosi, G. et al. Structural and spectroscopic properties of 2-thiophenecarboxaldehyde 2-thienylhydrazone. Journal of Crystallographic and Spectroscopic Research 19, 93–98 (1989). https://doi.org/10.1007/BF01160846

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  • DOI: https://doi.org/10.1007/BF01160846

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