Skip to main content
SpringerLink
Log in

X-ray structural investigation of 5,13-epoxy-3β-hydroxy-lactara-2(9),5,7(13)-trien-4,8-dion

  • Published:
Journal of Crystallographic and Spectroscopic Research Aims and scope Submit manuscript

Abstract

5,13-Epoxy-3β-hydroxy-lactara-2(9),5,7(13)-trien-4,8-dion was investigated by X-ray diffractometric methods. The compound is orthorhombic:P212121,a=7.677(1),b=11.244(2),c=15.277(2) Å andZ=4. The structure was solved by direct methods and refined by full-matrix least-squares, givingR=0.0387 for 1522 observed reflections. An internal hydrogen bond of medium strength was registered in the molecular structure.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

References

  • Daniewski, W. M., Gumułka, M., Ptaszyńska, K., Skibicki, P., Fronza, G., and Vidari, G. (1989)Bull. Acad. Polon. Sci. Ser. Sci. Chim. 37, 283.

    Google Scholar 

  • Daniewski, W. M., Gumułka, M., Skibicki, P., Jacobsson, U., and Norin, T. (1987)Bull. Acad. Polon. Sci. Ser. Sci. Chim. 35, 251.

    Google Scholar 

  • Daniewski, W. M. Gumułka, M, Skibicki, P., Krajewski, J. W., and Gluziński, P. (1990)Phytochemistry in press.

  • Daniewski, W. M., Kroszczyński, W., Skibicki, P., De Bernardi, M., Fronza, G., Vidari, G., and Vita-Finzi, P. (1988)Phytochemistry 27, 187.

    Google Scholar 

  • Magnusson, G., Thoren, S., Dahmen, J., and Leander, K. (1974)Acta Chem. Scand. B 28, 841.

    Google Scholar 

  • Nawrot, J., Błoszyk, E., Grabarczyk, H., Drożdz, B., Daniewski, W. M., and Holub, M. (1983)Pr. Naukowe 10R 25, 91.

    Google Scholar 

  • Sheldrick, G. M. (1976)Shelx -76. Program for Crystal Structure Determination and Refinement (University of Cambridge, England). 400-Atomic Version (Ch. Weizman Institute of Science, Rehovot, Israel, 1979); implemented on IBM PC/AT (1987).

    Google Scholar 

  • Sheldrick, G. M. (1985) in G. M. Sheldrick, C. Krüger, and R. Goddard (eds.),Crystallographic Computing 3 (Oxford University Press), pp. 175–189.

Download references

Author information

Authors and Affiliations

  1. Institute of Organic Chemistry, Polish Academy of Sciences, 01-224, Warszawa, Poland

    W. M. Daniewski, P. Gluziński, J. W. Krajewski & P. Skibicki

Authors
  1. W. M. Daniewski
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. P. Gluziński
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. J. W. Krajewski
    View author publications

    You can also search for this author in PubMed Google Scholar

  4. P. Skibicki
    View author publications

    You can also search for this author in PubMed Google Scholar

Rights and permissions

Reprints and permissions

About this article

Cite this article

Daniewski, W.M., Gluziński, P., Krajewski, J.W. et al. X-ray structural investigation of 5,13-epoxy-3β-hydroxy-lactara-2(9),5,7(13)-trien-4,8-dion. Journal of Crystallographic and Spectroscopic Research 21, 407–410 (1991). https://doi.org/10.1007/BF01160653

Download citation

  • Received:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF01160653

Keywords

Search

Navigation