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Über Fluorphenyliminophosphorsäuretrichloride

  • Anorganische, Struktur- und Physikalische Chemie
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Monatshefte für Chemie / Chemical Monthly Aims and scope Submit manuscript

Zusammenfassung

Die normaleKirsanov-Reaktion von fluorsubstit. Anilinen liefert Fluorphenyliminophosphorsäuretrichloride. Die Ammonolyse dieser Verbindungen führt zu Biphosphoniumchloriden der allgemeinen Form [RNH−P(NH2)2]2N+Cl−. Die IR-,19F- und31P-NMR-Spektren werden mitgeteilt und diskutiert.

Abstract

The normalKirsanov reaction of fluor-substituted anilines yields fluorinated N-phenyl-trichlorophosphineimines, which on ammonolysis give the corresponding bis(phosphoranylidene) ammonium chlorides [RNH−P(NH2)2]2N+Cl−. IR-,19F- and31P-NMR-spectra are reported and discussed.

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Authors and Affiliations

  1. Institut für Anorganische Chemie der Technischen Hochschule Wien, Wien, Österreich

    K. Utvary & M. Bermann

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  1. K. Utvary
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  2. M. Bermann
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Utvary, K., Bermann, M. Über Fluorphenyliminophosphorsäuretrichloride. Monatshefte für Chemie 99, 2369–2377 (1968). https://doi.org/10.1007/BF01154351

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  • DOI: https://doi.org/10.1007/BF01154351

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