Abstract
The first representative of perhydro-1,3-dioxa-6-azocines, 8,10-dimethyl-7,13-dioxa-10-azaspiro[5.7]tridecane, was synthesized by the reaction of 4-methyl-1-oxa-4-azaspiro[4.5]decane with propylene oxide. The structure of the compound has been confirmed by IR and1H and13C NMR spectroscopy and mass spectrometry.
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References
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Translated fromIzvestiya Akademii Nauk. Seriya Khimicheskaya, No. 9, pp. 1838–1839, September, 1995.
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Kukharev, B.F. 8,10-Dimethyl-7,13-dioxa-10-azaspiro[5.7]tridecane — the first representative of perhydro-1,3-dioxa-6-azocines. Russ Chem Bull 44, 1769–1770 (1995). https://doi.org/10.1007/BF01151310
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DOI: https://doi.org/10.1007/BF01151310