Abstract
S-Methyl-N-phenyl-iminothiocarbonic acid-tri-O.O′.O″-isopropylsilicic acid anhydride,1 is obtained from the reaction of phenyl isocyanate and methylthiotriiso-propoxysilan.1 readily hydrolyses forming S-methylthiocarbanilide. Substances are characterized by their mass and1H-NMR spectra.
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A. Meller undG. Beer, unveröffentlicht.
Vergleiche:Beilstein, Handbuch der Org. Chem., 4. Aufl.,12, S. 394 (1929).
Vergleiche:J. W. Emsley, J. Feeney undL. H. Sutcliffe, High Resolution NMR-spectroscopy, Vol.2, S. 1124, 1121. Oxford: Pergamon Press. 1966.
Vergleiche:Beilstein, Handbuch der Org. Chem., 4. Aufl.,12, S. 386 (1929).
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Beer, G., Meller, A. & Wojnowska, M. Über die Einschiebung von Phenylisocyanat in eine Silicium-Schwefelbindung. Monatshefte für Chemie 106, 567–569 (1975). https://doi.org/10.1007/BF01150539
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DOI: https://doi.org/10.1007/BF01150539