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Structure of the product of the complete hydrolysis of 1,2-bisdiazoacetylethane

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Bulletin of the Academy of Sciences of the USSR, Division of chemical science Aims and scope

Conclusions

The product of the complete hydrolysis of 1,2-bisdiazoacetylethane in aqueous HClO4, is 2,5-dioxo-1,6-hexanediol, whose structure was established by x-ray diffraction structural and analysis. UV spectroscopy indicates that this compound does not undergo keto-equal tautomerism characteristic forα-hydroxy ketone.

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Literature cited

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Authors and Affiliations

  1. Division of the Institute of Chemical Physics, Academy of Sciences of the USSR, Chernogolovka

    R. M. Lobkovskaya, L. I. Kirkovskii, V. G. Kartsev & R. P. Shibaeva

Authors
  1. R. M. Lobkovskaya
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  2. L. I. Kirkovskii
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  3. V. G. Kartsev
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  4. R. P. Shibaeva
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Additional information

Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 5, pp. 1184–1187, May, 1985.

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Lobkovskaya, R.M., Kirkovskii, L.I., Kartsev, V.G. et al. Structure of the product of the complete hydrolysis of 1,2-bisdiazoacetylethane. Russ Chem Bull 34, 1083–1086 (1985). https://doi.org/10.1007/BF01142807

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  • DOI: https://doi.org/10.1007/BF01142807

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