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Preferential chemical etching of terrestrial And lunar olivines

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Abstract

A new chemical etching technique has been developed to study defect structures in terrestrial and lunar olivine crystals. Dislocations, low-angle dislocation boundaries, dislocation arrays and pile-ups have been observed on the (010, (100), and (001) faces of both polished and cleaved naturally deformed single crystal olivine, on various orientations of crystals in dunite, and in an experimentally deformed olivine crystal. Etching of Apollo 12 igneous rocks revealed dislocations and radiation damage tracks in lunar olivine. Dislocation etching of the (001) face of olivine is reported for the first time in this paper.

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References

  • Amelinckx, S.: Etch pits and dislocations along grain boundaries, slip lines and polygonization walls. Acta Met.2, 848–853 (1954)

    Google Scholar 

  • Baranova, G. K., Nadgornyi, E. M.: Kinetics of polishing and etching crystals of sodium chloride. Soviet Phys.-Cyst.16, 506–509 (1971)

    Google Scholar 

  • Baranova, G. K., Nadgornyi, E. M.: Kinetics of polishing and etching sodium chloride crystals. II. Soviet Phys.-Cryst.17, 772–774 (1973)

    Google Scholar 

  • Bernas, B. A.: A new method for decomposition and comprehensive analysis of silicates by atomic absorption spectrometry. Anal. Chem.40, 1682–1686 (1968)

    Google Scholar 

  • Boland, J. N., McLaren, A. C., Hobbs, B. E.: Dislocations associated with optical features in naturally deformed olivines. Contr. Mineral. and Petrol.30, 53–63 (1971)

    Google Scholar 

  • Crozaz, G., Haack, U, Hair, M., Maurette, M., Walker, R., Woolum, D.: Nuclear track studies of ancient solar radiations and dynamic lunar surface processes. Geochim. Cosmochim. Acta, Suppl.1, 3, 2543–2558 (1971)

    Google Scholar 

  • Fleischer, R. L., Price, P. B.: Techniques for geological dating of minerals by chemical etching of fission fragment tracks. Geochim. Cosmochim. Acta28, 1705–1714 (1964)

    Google Scholar 

  • Gilman, J. J., Johnston, W. G.: Observations of glide and climb in lithium fluoride crystals. J. Appl. Phys.27, 1018–1022 (1956)

    Google Scholar 

  • Green, H. W., Radcliffe, S. V.: Dislocation mechanisms in olivine and flow in the upper mantle. Earth Plan. Sci. Lett.15, 239–247 (1972)

    Google Scholar 

  • Grossman, J. J., Ryan, J. A., Mukherjee, N. R., Wegner, M. W.: Microchemical, microphysical and adhesive properties of lunar material. Proc. Apollo 11 Lunar Sci. Conf., Geochim. Cosmochim. Acta, Suppl.1, 3, 2171–2181. New York, London: Pergamon 1970

    Google Scholar 

  • Grossman, J. J., Ryan, J. A., Mukherjee, N. R., Wegner, M. W.: Microchemical and microphysical properties of lunar material II. Proc. Second Lunar Sci. Conf.3, 2153–2164. Cambridge, Mass.: MIT Press 1971

    Google Scholar 

  • Gutamanas, É. Yu., Nadgornyi, É. M.: Selective etching of dislocations in rubidium iodide crystals. Soviet Phys.-Cryst.13, 85–89 (1968)

    Google Scholar 

  • Honess, A. P.: The nature, origin and interpretation of etch figures on crystals., p. 14–74. New York: Wiley 1927

    Google Scholar 

  • Horn, F. H.: Screw dislocations, etch figures and holes. Phil. Mag.43, 1210–1213 (1952)

    Google Scholar 

  • Horn, P., Maurette, M.: Ein Beitrag zum Ätzverhalten des Olivins. Neues Jahrb. Mineral., Monatsh.1, 170–178 (1967)

    Google Scholar 

  • Huang, W. H., Keller, W. D.: Dissolution of rock forming silicates in organic acids. Am. Mineralogist55, 2076–2094 (1970)

    Google Scholar 

  • Ives, M. B., McAusland, D. D.: On the slope of etch pits. Surface Science12, 189–207 (1968)

    Google Scholar 

  • Johnston, W. G.: Dislocation etch pits in non-metallic crystals with bibliography. In: Progress in ceramic science, vol. 2, ed. J. E. Burke, p. 1–75. New York: Pergamon Press 1962

    Google Scholar 

  • Kirby, S. H., Wegner, M. W.: Dislocation substructure of mantle-derived olivine as revealed by selective chemical etching. Trans. Am. Geophys. Union54, 452 (1973)

    Google Scholar 

  • Krishnaswami, S., Lal, D., Prabhu, N., Tamhane, A. S.: Olivines: Revelation of tracks of charged particles. Science174, 287–291 (1971)

    Google Scholar 

  • Lundström, I.: Etch-pattern and albite twinning in two plagioclases. Arkiv för Mineralogi Och Geologi5, No.7, 63–91 (1970)

    Google Scholar 

  • Maurette, M.: Étude des traces d'ions lourds dans les minéraux naturels d'origine terrestre et extra-terrestre. Bull. Soc. Franc. Mineral. Crist.89, 41–79 (1966)

    Google Scholar 

  • Moran, P. R.: Dislocation etch techniques for some alkali halide crystals. J. Appl. Phys.29, 1768–1769 (1958)

    Google Scholar 

  • Nicolas, A., Bouchez, J. L., Boudier, F., Mercier, J. C.: Textures, structures and fabrics due to solid state flow in some European lherzolites. Tectonophysics12, 55–86 (1971)

    Google Scholar 

  • Phakey, P., Dollinger, G., Christie, J. M.: Transmission electron microscopy of experimentally deformed olivine crystals. In: Flow and fracture of rocks. Geophys. Monograph16, 117–138. Amer. Geophys. Union (1972)

    Google Scholar 

  • Regel, V. R., Urusovskaya, A. A., Kolomiichuk, V. N.: Revealing the emergence of dislocations on the surface of a crystal by the etch method. Soviet. Phys.-Cryst.4, 895–917 (1960)

    Google Scholar 

  • Sapozhnikov, D. G. (Ed.): Experimental research into the decomposition of minerals by organic acids. Akademiya Nauk SSSR. Institut Geologii Rudnykh Mestorozhdeniy, Petrografii, Mineralogii i Geokhimii, Moscow, Izd-vo “Nauka” (1968), 177 p

    Google Scholar 

  • Sears, G. W.: Dislocation etchings. J. Chem. Phys.32, 5, 1317–1322 (1960)

    Google Scholar 

  • Talvitie, N. A.: Determination of quartz in presence of silicates using phosphoric acid. Anal. Chem.23, 623–626 (1951)

    Google Scholar 

  • Wegner, M. W., Grossman, J. J.: Dislocation etching of naturally deformed olivine. Trans. Am. Geophys. Union50, 676 (1969)

    Google Scholar 

  • Young, C. III: Dislocations in the deformation of olivine. Am. J. Sci.267, 841–852 (1969)

    Google Scholar 

  • Young, D. A.: Etching of radiation damage in lithium fluoride. Nature4632, 375–377 (1958)

    Google Scholar 

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Wegner, M.W., Christie, J.M. Preferential chemical etching of terrestrial And lunar olivines. Contr. Mineral. and Petrol. 43, 195–212 (1974). https://doi.org/10.1007/BF01134836

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