Conclusions
Reaction of thioepichlorohydrin and 3-chlorothietane with diethyl-thiophosphate salts gives only the thio esters of diethyl-phosphoric acid. Reaction with thiocyanate salts gives isothiocyanates in addition to thiocyanates.
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Literature cited
O. N. Nuretdinova and B. A. Arbuzov, Izv. AN SSSR, Ser. Khim., 2318 (1968).
O. N. Nuretdinova, B. A. Arbuzov, and F. F. Guseva, Izv. AN SSSR, Ser. Khim., 1881 (1970).
B. A. Arbuzov and O. N. Nuretdinova, Izv. AN SSSR, Ser. Khim., 2594 (1971).
O. N. Nuretdinova and B. A. Arbuzov, Izv. AN SSSR, Ser. Khim., 550 (1975).
O. N. Nuretdinova and B. A. Arbuzov, Izv. AN SSSR, Ser. Khim., 145 (1970).
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Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 3, pp. 662–665, March, 1973.
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Nuretdinova, O.N., Guseva, F.F. Reacticn of thioepichlorohydrin and 3-chlorothietane with salts of diethylthiophosphoric and thiocyanic acids. Russ Chem Bull 25, 647–649 (1976). https://doi.org/10.1007/BF01106673
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DOI: https://doi.org/10.1007/BF01106673