Chemistry of Heterocyclic Compounds

, Volume 5, Issue 1, pp 121–122 | Cite as

Synthesis of some sym-triazole derivatives

  • S. S. Novikov
  • V. M. Brusnikina
  • V. A. Rudenko
Article

Abstract

3,5-Di(hydroxyalkyl) derivatives of 4-amino-1,2,4-triazole and the corresponding derivatives of 1,2,4-triazole obtained by diazotizing them are converted by reaction with SOCl2 into the hydrochlorides of 4-amino-3,5-di(chloroalkyl)-1,2,4-triazoles and 3,5-di(chloroalkyl)-1, 2,4-triazoles. The dinitrate of 3,5-di(hydroxymethyl)-1,2,4-triazole has been prepared. When the cyanohydrazide of glycolic acid is heated with hydrazine hydrate, 4,5-diamino-3-hydroxymethyl-1, 2,4-triazole is formed.

Keywords

Hydrate Organic Chemistry Hydrochloride Hydrazine Triazole 

References

  1. 1.
    V. M. Brusnikina, S. S. Novikov, and V. A. Rudenko, Izv. AN SSSR, OKhN, 1681, 1963.Google Scholar

Copyright information

© Consultants Bureau 1971

Authors and Affiliations

  • S. S. Novikov
    • 1
  • V. M. Brusnikina
    • 1
  • V. A. Rudenko
    • 1
  1. 1.Zelinskii Institute of Organic Chemistry AS USSRMoscow

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