Conclusions
The silylation of 5-chloromethyl-2-isoxazoline-3-carboxylic acid with the usual silylating agents leads to the corresponding trimethylsilyl ester, which when heated is converted to 4-chloro-3-trimethylsiloxybutyronitrile.
Literature cited
R. Rambaud and M. Vesierre, Bull. Soc. Chim. France,1956, 783.
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Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 12, pp. 2818–2819, December, 1981.
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Ioffe, S.L., Kuznetsov, Y.D. & Tartakovskii, V.A. Unusual transfoemation of trimethylsilyl ester of 5-chloromethyl-2-isoxazoline-3-carboxylic acid. Russ Chem Bull 30, 2350–2351 (1981). https://doi.org/10.1007/BF00963710
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DOI: https://doi.org/10.1007/BF00963710