Conclusions
The reaction of the methyl ester of 3-phenyl-3-chloro-2-ketopropionic acid with mercaptoethanol and 1,2-dithioglycol gives derivatives of oxathiine and dithiine. The oxidation of these products gives the corresponding sulfones.
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Literature cited
V. A. Mamedov and I. A. Nuretdinov, Izv. Akad. Nauk SSSR, Ser. Khim., 2856 (1987).
N. N. Mel'nikov, K. V. Novozhilov, and T. N. Pylova, Handbook for Chemical Means for the Protection of Plants [in Russian], Izd. Khimiya, Moscow (1980), p. 227; G. S. Gruzdev (ed.), Chemical Plant Protection [in Russian], Agropromizdat, Moscow (1987), p. 272.
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Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 7, pp. 1670–1672, July, 1988.
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Mamedov, V.A., Nuretdinov, I.A. Synthesis of esters of oxathiinecarboxylic and dithiinecarboxylic acids and their derivatives. Russ Chem Bull 37, 1485–1486 (1988). https://doi.org/10.1007/BF00962768
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DOI: https://doi.org/10.1007/BF00962768