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Synthesis of 2-amino-4,4-bis(trifluoromethyl)-3-cyano-4,5-dihydro-1H-1,5-benzodiazepine

  • K. V. Komarov
  • N. D. Chkanikov
  • S. V. Sereda
  • M. Yu. Antipin
  • Yu. T. Struchkov
  • A. F. Kolomiets
  • A. V. Fokin
Brief Communications

Conclusions

The reaction of 1,2-phenylenediamine with 2,2-bis(trifluoromethyl)-1,1-dicyanoethylene leads to the formation of 2-amino-4,4-bis(trifluoromethyl)-3-cyano-4,5-dihydro-lH-l,5-benzodiazepine, whose structure was established by x-ray diffraction analysis.

Keywords

Diffraction Analysis Trifluoromethyl Dicyanoethylene 
These keywords were added by machine and not by the authors. This process is experimental and the keywords may be updated as the learning algorithm improves.

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Literature cited

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    W. J. Middleton, J. Org. Chem., 1402 (1965).Google Scholar
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    W. J. Middleton and E. M. Bingham, J. Fluor. Chem., 397 (1982).Google Scholar
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    M. Burke-Laing and M. Laing, Acta Crystallogr.,32, 3216 (1976).Google Scholar
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    M. Shenk (ed.), Computing in Crystallography, University Press, Delft (1978).Google Scholar

Copyright information

© Plenum Publishing Corporation 1989

Authors and Affiliations

  • K. V. Komarov
    • 1
  • N. D. Chkanikov
    • 1
  • S. V. Sereda
    • 1
  • M. Yu. Antipin
    • 1
  • Yu. T. Struchkov
    • 1
  • A. F. Kolomiets
    • 1
  • A. V. Fokin
    • 1
  1. 1.A. N. Nesmeyanov Institute of Heteroorganic CompoundsAcademy of Sciences of the USSRMoscow

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