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Reaction of 1-bromo-2-acylacetylenes with thiobenzhydrazide

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Bulletin of the Academy of Sciences of the USSR, Division of chemical science Aims and scope

Conclusions

The reactions of 1-bromo-2-acylacetylenes with thiobenzhydrazide at from −10 to −30°C in ether, acetonitrile, methanol without catalyst, or methanol in the presence of triethylamine gave 2-acylmethyl-5-phenyl-1,3,4-thiadiazoles and their hydrobromide salts.

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Literature cited

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Authors and Affiliations

  1. Irkutsk Institute of Organic Chemistry, Siberian Branch, Academy of Sciences of the USSR, USSR

    T. E. Glotova, A. S. Nakhmanovich, T. N. Komarova & M. V. Sigalov

Authors
  1. T. E. Glotova
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  2. A. S. Nakhmanovich
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  3. T. N. Komarova
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  4. M. V. Sigalov
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Additional information

Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 11, pp. 2637–2638, November, 1988.

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Glotova, T.E., Nakhmanovich, A.S., Komarova, T.N. et al. Reaction of 1-bromo-2-acylacetylenes with thiobenzhydrazide. Russ Chem Bull 37, 2376–2377 (1988). https://doi.org/10.1007/BF00959905

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  • DOI: https://doi.org/10.1007/BF00959905

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