Conclusions
The five-membered heterocycle in the structure of 3-oxo-3-chloromethyl-2,3-dihydro-1,3-benzoxaphosphole is planar to within ±0.03 Å with the greatest (CPC)endo bond angle equal to 91.33(7)°.
Literature cited
V. A. Naumov and L. V. Vilkov, The Molecular Structures of Organophosphorus Compounds [in Russian], Nauka, Moscow (1986).
International Tables for X-Ray Crystallography, Vol. 3, Kynoch Press, Birmingham, England (1968), p. 276.
R. Taylor and O. Kennard, J. Am. Chem. Soc.,104, 5063 (1982).
A. N. Chekhlov, S. P. Ionov, A. N. Bovin, et al., Izv. Akad. Nauk SSSR, Ser. Khim., 2240 (1985).
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Translated from Izvestiya Akademii Nauk SSSR, Seriya Kkimicheskaya, No. 11, pp. 2630–2632, November, 1988.
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Chekhlov, A.N., Bovin, A.N., Tsvetkov, E.N. et al. Crystal and molecular structure of 3-oxo-3-chloromethyl-2,3-dihydro-1,3-benzoxaphosphole. Russ Chem Bull 37, 2369–2371 (1988). https://doi.org/10.1007/BF00959902
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DOI: https://doi.org/10.1007/BF00959902