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Synthesis and1H and31P NMR spectral characteristics of 2-substituted and 2,2-disubstituted 5-phenyl-5-thio-1,3,5-dioxaphosphorinanes

  • Organic Chemistry
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Bulletin of the Academy of Sciences of the USSR, Division of chemical science Aims and scope

Conclusions

Treatment of phenylbis(hydroxymethyl)phosphine sulfide with acetals and ketals gives the corresponding 2-substituted and 2,2-disubstituted 5-phenyl-5-thio-1,3,5-dioxaphosphorinanes in which the P-Phenyl substituent occupies an axial position.

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Authors and Affiliations

  1. A. E. Arbuzov Institute of Organic and Physical Chemistry, Kazan Branch of the Academy of Sciences of the USSR, USSR

    B. A. Arbuzov, O. A. Erastov, A. S. Ionkin & S. N. Ignat'eva

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  1. B. A. Arbuzov
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  2. O. A. Erastov
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  3. A. S. Ionkin
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  4. S. N. Ignat'eva
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Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 2, pp. 418–422, February, 1987.

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Arbuzov, B.A., Erastov, O.A., Ionkin, A.S. et al. Synthesis and1H and31P NMR spectral characteristics of 2-substituted and 2,2-disubstituted 5-phenyl-5-thio-1,3,5-dioxaphosphorinanes. Russ Chem Bull 36, 377–381 (1987). https://doi.org/10.1007/BF00959386

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  • DOI: https://doi.org/10.1007/BF00959386

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