Unusual transformations of arylhydrazonoyl chlorides of ethyl oxalate

  • M. O. Lozinskii
  • V. N. Bodnar
  • S. V. Konovalikhin
  • O. A. D'yachenko
  • L. O. Atovmyan
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Abstract

X-ray diffraction structural analysis, IR,13C NMR, and PMR spectroscopy was used to establish that the products of the reactions of arylhydrazonoyl chlorides of ethyl oxalate and sodium ethylate are 1,4-diaryl-3,6-dicarboethoxy-1,4-dihydro-1,2,4,5-tetrazines and 1-aryl-3-carboethoxy-4-arylhydrazono-5-pyrazolones.

Keywords

Sodium Spectroscopy Chloride Ethyl Structural Analysis 

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Literature cited

  1. 1.
    F. Enders, Methoden der Organischen Chemie, Vol. 10/2, Georg Thieme Verlag, Stuttgart (1967), pp. 340–520.Google Scholar
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    V. N. Bodnar, M. O. Lozinskii, and P. S. Pel'kis, Ukr. Khim. Zh.,48, No. 12, 1308 (1982).Google Scholar
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    V. I. Andrianov, Z. Sh. Safina, and B. L. Tarnopol'skii, Roentgen-75, Branch of the N. N. Semenov Institute of Chemical Physics, Academy of Sciences of the USSR, Chernogolovka (1975).Google Scholar

Copyright information

© Plenum Publishing Corporation 1991

Authors and Affiliations

  • M. O. Lozinskii
    • 1
    • 2
  • V. N. Bodnar
    • 1
    • 2
  • S. V. Konovalikhin
    • 1
    • 2
  • O. A. D'yachenko
    • 1
    • 2
  • L. O. Atovmyan
    • 1
    • 2
  1. 1.Institute of Organic ChemistryAcademy of Sciences of the Ukrainian SSRKiev
  2. 2.Branch of the N. N. Semenov Institute of Chemical PhysicsAcademy of Sciences of the USSRChernogolovka

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