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Structures of two modifications of 6,9-bis-pyridine-nidodecaborane(12)

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Bulletin of the Academy of Sciences of the USSR, Division of chemical science Aims and scope

Abstract

An x-ray diffraction structural analysis showed the molecular and crystal structures of two modifications of 6,9-bis-pyridine-nido-decaborane(12). The orientation of the pyridine rings relative to the ¦B10H12¦ unit proposed by Graybill and Hawthorne [1] was not confirmed for the crystalline states of B10H12(C5H5N)2.

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Literature cited

  1. B. M. Graybill and M. F. Hawthorne, J. Am. Chem. Soc.,83, 2673 (1961).

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  2. V. V. Volkov, K. G. Myakishev, O. G. Potapova, et al., Izv. Sib. Otd. Akad. Nauk SSSR, Ser. Khim. Nauk, No. 9, Issue 3, 20 (1988).

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  3. V. I. Andrianov, Kristallografiya,32, 228 (1987).

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Authors and Affiliations

  1. Institute of Inorganic Chemistry, Siberian Branch, Academy of Sciences of the USSR, Novosibirsk

    T. M. Polyanskaya, V. V. Volkov, V. I. Andrianov & E. A. Il'inchik

Authors
  1. T. M. Polyanskaya
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  2. V. V. Volkov
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  3. V. I. Andrianov
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  4. E. A. Il'inchik
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Additional information

Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 8, pp. 1905–1909, August, 1989.

The authors express their gratitude to S. T. Dunaev for synthesizing these compounds, to V. A. Shipachev for taking the UV spectra, and to N. V. Podberezskaya and L. A. Glinskaya for assistance in obtaining the diffractometric data.

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Polyanskaya, T.M., Volkov, V.V., Andrianov, V.I. et al. Structures of two modifications of 6,9-bis-pyridine-nidodecaborane(12). Russ Chem Bull 38, 1751–1754 (1989). https://doi.org/10.1007/BF00956968

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  • DOI: https://doi.org/10.1007/BF00956968

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