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A13C NMR specteal study of the complexation of aluminum diethyl chloride with pyridine

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Bulletin of the Academy of Sciences of the USSR, Division of chemical science Aims and scope

Conclusions

  1. 1.

    The reaction of diethylchloroaluminum with pyridine in benzene leads to a stable complex.

  2. 2.

    13C NMR spectroscopy was used to establish the intermediate state as an ion pair of the dimer of diethylchloroaluminum and one pyridine molecule.

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Literature cited

  1. V. M. Denisov, Dissertation, Leningrad (1977).

  2. S. I. Vinogradova, V. M. Denisov, and A. I. Kol'tsov, Zh. Obshch. Khim.,42, 1031 (1972).

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  3. G. Heublein, W. Kümpfel, and H. Schütz, Z. Chem.,18, 34 (1978).

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  4. H. Lehmkuhl and H. D. Kobs, Tetrahedron Lett., 2505 (1965).

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Authors and Affiliations

  1. Institute of High-Molecular-Weight Compounds, Academy of Sciences of the USSR, Leningrad

    H. Schütz, P. Halpap, V. M. Denisov, D. Staderman, G. Hartung, G. Heublein & A. I. Kol'tsov

  2. Chemistry Section, F. Schiller University, Jena, GDR

    H. Schütz, P. Halpap, V. M. Denisov, D. Staderman, G. Hartung, G. Heublein & A. I. Kol'tsov

Authors
  1. H. Schütz
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  2. P. Halpap
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  3. V. M. Denisov
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  4. D. Staderman
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  5. G. Hartung
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  6. G. Heublein
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  7. A. I. Kol'tsov
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Additional information

Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 3, pp. 684–685, March, 1986.

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Schütz, H., Halpap, P., Denisov, V.M. et al. A13C NMR specteal study of the complexation of aluminum diethyl chloride with pyridine. Russ Chem Bull 35, 625–626 (1986). https://doi.org/10.1007/BF00953242

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  • DOI: https://doi.org/10.1007/BF00953242

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