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Alkylation of difluoronitroethanol by epichlorohydrin

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Bulletin of the Academy of Sciences of the USSR, Division of chemical science Aims and scope

Conclusions

The reaction of 2,2-difluoro-2-nitroethanol with epichlorohydrin in alkaline medium gives 2,2-difluoro-2-nitroethyl glycidyl ether, whose yield is raised to 70% upon carrying out the reaction in the presence of formaldehyde.

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Literature cited

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Authors and Affiliations

  1. A. N. Nesmeyanov Institute of Heteroorganic Compounds, Academy of Sciences of the USSR, Moscow

    A. V. Fokin, V. I. Shevchenko & E. I. Lyubimova

Authors
  1. A. V. Fokin
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  2. V. I. Shevchenko
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  3. E. I. Lyubimova
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Additional information

Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 12, pp. 2865–2868, December, 1988.

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Fokin, A.V., Shevchenko, V.I. & Lyubimova, E.I. Alkylation of difluoronitroethanol by epichlorohydrin. Russ Chem Bull 37, 2586–2589 (1988). https://doi.org/10.1007/BF00952653

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  • DOI: https://doi.org/10.1007/BF00952653

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