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Conclusions

  1. 1.

    The stable 1,1-bis(trifluoromethyl)hydrazine was synthesized by the thermal decomposition of either tert-butyl bis(trifluoromethyl)carbamate or a solution of bis(trifluoromethyl) carbamic acid azide in the presence of water, and its reaction with perfluoro-2-aza-propene, bis(trifluoromethyl)ketene, and hexafluoroacetone was studied.

  2. 2.

    The dhydration of the adduct of 1,1-bis(trifluoromethyl)hydrazine with hexafluoroacetone by oleum gave hexafluoroacetone bis(trifluoromethyl)hydrazone, the first member of the perfluorohydrazones.

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Literature cited

  1. A. F. Gontar, É. G. Bykhovskaya, A. S. Vinogradov, and I. L. Knunyants, Izv. Akad. Nauk SSSR, Ser. Khim., 2632 (1981).

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Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 2, pp. 436–438, February, 1984.

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Bykhovskaya, É.G., Gontar', A.F. & Knunyants, I.L. 1,1-Bis(trifluoromethyl)hydrazine. Russ Chem Bull 33, 399–401 (1984). https://doi.org/10.1007/BF00951084

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  • DOI: https://doi.org/10.1007/BF00951084

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